Journal of Bionic Engineering ›› 2020, Vol. 17 ›› Issue (2): 393-404.doi: 10.1007/s42235-020-0032-5

• • 上一篇    

Characterization of Novel Lignocellulosic Spinifex littoreus Fibers and Their Composites

Milan Soosai1, Christopher Thankian2, Winowlin Jappes Jebas Thangiah3, Rajini Nagarajan3*,
Mayandi Kalimuthu3, Sikiru Oluwarotimi Ismail4, Faruq Mohammad5
  

  1. 1. Department of Mechanical Engineering, Cape Institute of Technology, Levengipuram, Tirunelveli 627114, Tamil Nadu, India
    2. Department of Mechatronics Engineering, Kamaraj College of Engineering & Technology Vellakulam,
    Madurai dist-622701, Tamil Nadu, India
    3. Centre for Composite Materials, Department of Mechanical Engineering, Kalasalingam University, Krishnankoil,
    Virudhunagar 626 126, Tamil Nadu, India
    4. Centre for Engineering Research, Department of Engineering, School of Engineering and Computer Science,
    University of Hertfordshire, Hatfield, Hertfordshire AL10 9AB, UK
    5. Surfactants Research Chair, Department of Chemistry, College of Science, King Saud University, Riyadh 11451,
    Kingdom of Saudi Arabia

  • 收稿日期:2019-05-29 修回日期:2019-12-05 接受日期:2020-02-10 出版日期:2020-03-10 发布日期:2020-04-08
  • 通讯作者: Rajini Nagarajan E-mail:rajiniklu@gmail.com
  • 作者简介:Milan Soosai1, Christopher Thankian2, Winowlin Jappes Jebas Thangiah3, Rajini Nagarajan3*, Mayandi Kalimuthu3, Sikiru Oluwarotimi Ismail4, Faruq Mohammad5

Characterization of Novel Lignocellulosic Spinifex littoreus Fibers and Their Composites

Milan Soosai1, Christopher Thankian2, Winowlin Jappes Jebas Thangiah3, Rajini Nagarajan3*,#br# Mayandi Kalimuthu3, Sikiru Oluwarotimi Ismail4, Faruq Mohammad5#br#   

  1. 1. Department of Mechanical Engineering, Cape Institute of Technology, Levengipuram, Tirunelveli 627114, Tamil Nadu, India
    2. Department of Mechatronics Engineering, Kamaraj College of Engineering & Technology Vellakulam,
    Madurai dist-622701, Tamil Nadu, India
    3. Centre for Composite Materials, Department of Mechanical Engineering, Kalasalingam University, Krishnankoil,
    Virudhunagar 626 126, Tamil Nadu, India
    4. Centre for Engineering Research, Department of Engineering, School of Engineering and Computer Science,
    University of Hertfordshire, Hatfield, Hertfordshire AL10 9AB, UK
    5. Surfactants Research Chair, Department of Chemistry, College of Science, King Saud University, Riyadh 11451,
    Kingdom of Saudi Arabia

  • Received:2019-05-29 Revised:2019-12-05 Accepted:2020-02-10 Online:2020-03-10 Published:2020-04-08
  • Contact: Rajini Nagarajan E-mail:rajiniklu@gmail.com
  • About author:Milan Soosai1, Christopher Thankian2, Winowlin Jappes Jebas Thangiah3, Rajini Nagarajan3*, Mayandi Kalimuthu3, Sikiru Oluwarotimi Ismail4, Faruq Mohammad5

摘要: This innovative work presents mechanical, physical and chemical characterization and analysis of newly extracted fiber from natu-rally resourced plant stem, named Spinifex littoreus fibers (SLF). This is a novel natural, biodegradable and sustainable reinforcement for an improved composite. Initially, the chemical constituents of SLF, such as cellulose, lignin, moisture and wax content were studied. The raw SLF surfaces were modified by chemical treatment with sodium hydroxide (NaOH), calcium hydroxide (Ca(OH)2) and silane. A polyester matrix was reinforced with all the treated SLF, before the mechanical properties (tensile strengths) of the composites were determined. Among all the surface chemically treated SLF/polyester composite samples, the Ca(OH)2 treated sample exhibited the highest tensile strength. Further microscopic examination was carried out to validate this result. Also, this analysis established the mechanism of failure of the tensile fractured composite samples, using Scanning Electron Microscope (SEM), among other techniques.


关键词: cellulosic fiber, Spinifex littoreus fibers, XRD, FTIR, SEM, tensile strength

Abstract: This innovative work presents mechanical, physical and chemical characterization and analysis of newly extracted fiber from natu-rally resourced plant stem, named Spinifex littoreus fibers (SLF). This is a novel natural, biodegradable and sustainable reinforcement for an improved composite. Initially, the chemical constituents of SLF, such as cellulose, lignin, moisture and wax content were studied. The raw SLF surfaces were modified by chemical treatment with sodium hydroxide (NaOH), calcium hydroxide (Ca(OH)2) and silane. A polyester matrix was reinforced with all the treated SLF, before the mechanical properties (tensile strengths) of the composites were determined. Among all the surface chemically treated SLF/polyester composite samples, the Ca(OH)2 treated sample exhibited the highest tensile strength. Further microscopic examination was carried out to validate this result. Also, this analysis established the mechanism of failure of the tensile fractured composite samples, using Scanning Electron Microscope (SEM), among other techniques.


Key words: cellulosic fiber, Spinifex littoreus fibers, XRD, FTIR, SEM, tensile strength